| 谢若男,杨满琴,王丽,等.痹痛丸的质量控制研究[J].安徽医药,2017,21(4):643-645. |
| 痹痛丸的质量控制研究 |
| Quality standard research of Bitong pill |
| 投稿时间：2016-10-20 |
| DOI： |
| 中文关键词: 痹痛丸 质量标准 薄层色谱法 高效液相色谱法 |
| 英文关键词: Bitong pill Quality standard TLC HPLC |
| 基金项目:安徽省卫生和计划生育委员会中医药科研课题项目(2014zy15)痹痛丸的质量控制研究谢若男,杨满琴,王丽,徐玥玮,高晓明 (安徽中医药大学第二附属医院药学部,安徽 合肥 230061)痹痛丸的质量控制研究 谢若男,杨满琴,王丽,徐玥玮,高晓明 Quality standard research of Bitong pill XIE Ruonan,YANG Manqin,WANG Li,XU Yuewei,GAO Xiaoming |
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| 中文摘要: |
| 目的 建立痹痛丸的质量标准。方法 采用薄层色谱法(TLC)对痹痛丸中防风、蜜麻黄进行定性鉴别；采用高效液相色谱法(HPLC)对痹痛丸中的芍药苷进行含量测定。结果 采用TLC法均能检出防风、蜜麻黄中的特征斑点,分离度好；HPLC法测出芍药苷在5.91~59.1 mg·L-1范围内与吸收峰面积值呈良好的线性关系(r=0.999 9)。平均回收率为98.13%,RSD=1.01%(n=9)。结论 建立的质量标准方法简便、重现性好,可用于痹痛丸的质量控制。 |
| 英文摘要: |
| Objective To establish a quality standard for Bitong pill.Methods Saposhnikoviae Radix,Ephedrae Herba were identified by TLC.The content of Paeoniflorin was measured by HPLC.Results The special spot of Saposhnikoviae Radix,Ephedrae Herba were identified by TLC and TLC has good separation.The linear range of Paeoniflorin was measured by HPLC within 5.91~59.1 mg·L-1,and the average recovery was 98.13% and RSD 1.01%(n=9).Conclusions The method is simple and reproducible,and can be used for the quality control of Bitong pill. |
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