| 童学飞,吴雪,杜学辉.骨痹息痛巴布膏的质量标准研究[J].安徽医药,2017,21(1):24-26. |
| 骨痹息痛巴布膏的质量标准研究 |
| Quality standard of gubixitong babu plaster |
| 投稿时间：2016-01-29 |
| DOI： |
| 中文关键词: 骨痹息痛巴布膏 质量标准 薄层色谱法 高效液相色谱法 |
| 英文关键词: Gubixitong Babu Plaster Quality standard TLC HPLC |
| 基金项目:2015年十堰市科学技术研究与开发项目计划(15Y66) |
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| 中文摘要: |
| 目的 建立骨痹息痛巴布膏的质量标准。方法 采用薄层色谱法对其中的青风藤和延胡索等药材进行了鉴别,高效液相色谱法对其中的盐酸巴马汀进行含量测定。色谱柱:InertSustain C18 (5 μm,4.6 mm×250 mm)；流动相:乙腈-0.4%磷酸溶液(30∶70)；检测波长:345 nm；柱温:30 ℃；流速:1 mL·min-1。结果 制定了骨痹息痛巴布膏中青风藤和延胡索等药材的薄层鉴别方法和盐酸巴马汀的含量测定方法。结论 该分析方法简便可靠、重现性好,基本可控制骨痹息痛巴布膏的质量。 |
| 英文摘要: |
| Objective To establish the quality standard of Gubixitong Babu Plaster. Methods TLC was adopted to identify the medicinal materials of Sinomenii Caulis and Corydalis in Gubixitong Babu Plaster.HPLC was applied to determinate the content of palmatine hydrochloride in Gubixitong Babu Plaster.The InertSustain C18 (5 μm,4.6 mm×250 mm) was adopted with the Mobile Phase of acetonitrile-0.4% phosphoric acid solution (30∶70).The detection wavelength was set at 345 nm with a column tempetature of 30 ℃ and a flow rate of 1 mL·min-1. Results TLC of identifying the medicinal materials of Sinomenii Caulis and Corydalis and HPLC of determining the content of palmatine hydrochloride in Gubixitong Babu Plaster were formulated. Conclusions The method is simple,reliable and reproducible for the quality control of Gubixitong Babu Plaster. |
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