| 任路路,姚大洋,任莹,等.五味子降酶胶囊质量控制研究[J].安徽医药,2022,26(4):676-679. |
| 五味子降酶胶囊质量控制研究 |
| Study on quality control of Schisandra Transaminase reduction capsule |
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| DOI：10.3969/j.issn.1009-6469.2022.04.008 |
| 中文关键词: 中草药 五味子属 色谱法，高效液相 色谱法，薄层 五味子降酶胶囊 板蓝根 五味子醇甲 |
| 英文关键词: Drugs,chinese herbal Schisandra Chromatography, high pressure liquid Chromatography, thin layer Schisan dra transaminase reduction capsule Radix isatidis Schisandrin A |
| 基金项目: |
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| 中文摘要: |
| 目的探讨五味子降酶胶囊的质量控制方法。方法采用薄层色谱法( TLC)鉴别五味子降酶胶囊中的五味子、板蓝根；采用高效液相色谱法(HPLC)测定五味子中五味子醇甲的含量。结果薄层鉴别斑点清晰，分离效果好，专属性强；含量测定中五味子醇甲在 0.033 37～0.533 92 μg范围内，与峰面积线性关系良好(r=0.999 5)。结论方法操作简单，专属性和重现性良好，可作为五味子降酶胶囊的质量控制方法。 |
| 英文摘要: |
| Objective To explore the quality control method of Schisandra Transaminase reduction capsule.Methods The thin lay er chromatography (TLC) method was used to identify qualitation for Schisandra chinensis and Radix isatidis in Schisandra Transami nase reduction capsule; high performance liquid chromatography (HPLC) method was used to determine the contents of Schisandrin Ain Schisandra chinensis.Results The spot was clear in TLC identification with good separation effect and strong specificity. The con tent of Schisandrin A had a good linear relation with peak area (r=0.999 5), when ranged from 0.033 37 to 0.533 92 μg.Conclusion The method is simple with good specificity and reproducibility, and can be used as the quality control for Schisandra Transaminase re duction capsule. |
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